Analysis
XRD Phase Analysis
X-ray diffraction for crystalline phase identification, quantitative phase analysis, crystallite size and degree of crystallinity in powders and solids.
In short
X-ray diffraction for crystalline phase identification, quantitative phase analysis, crystallite size and degree of crystallinity in powders and solids. XRD phase analysis is performed on an Anton Paar XRDynamic 500 powder diffractometer. Crystallite size and microstrain are derived from peak broadening using Scherrer or Williamson–Hall analysis, and percentage crystallinity from the amorphous and crystalline peak areas.
XRD phase analysis is performed on an Anton Paar XRDynamic 500 powder diffractometer. The diffraction pattern is matched against the ICDD PDF database to identify the crystalline phases present, and phase fractions are calculated by Rietveld refinement or the reference intensity ratio (RIR) method. Crystallite size and microstrain are derived from peak broadening using Scherrer or Williamson–Hall analysis, and percentage crystallinity from the amorphous and crystalline peak areas. The service answers whether a synthesis product has converted to the target phase, whether impurity phases are present, which polymorph is present, how calcination or milling has changed the structure, and whether batches are consistent. It addresses ceramics, cement and minerals, metal powders, catalysts, battery materials, pharmaceuticals and nanomaterials as well as academic research groups.
What you receive
Diffraction patterns (2θ–intensity) with phase matches marked and peak list
ICDD PDF card numbers for identified phases and quantitative phase fractions
Crystallite size, microstrain and percentage crystallinity (on request)
Method summary covering radiation, optics, scan range and step time
Raw data (XRDML/CSV) and PDF report
How it works
Request and scoping
Expected phases, sample form, required outputs (qualitative/quantitative, crystallite size) and scan range are agreed with you.
Sample reception and preparation
Samples are logged; powders are ground and sieved where needed and loaded into holders in a way that minimises preferred orientation.
Measurement
The diffraction pattern is collected over the chosen 2θ range with a step time sufficient for the counting statistics required by quantitative analysis.
Reporting
Results are presented in the standard analysis report; supporting technical documentation is shared on request.
Pricing
€140
per sample
| 1+ | €140 |
| 5+ | €126 |
| 10+ | €112 |
Lead time 3–7 business days
Final pricing depends on sample count, preparation and reporting scope. You receive an itemised proposal.
Prices are a guide and may change with any additional requests. Our team will contact you to confirm the scope and the final price.Request this service
Describe your sample and the decision it supports. We reply with a technical proposal.
Request analysisInstruments used
- XRD
- Anton Paar XRDynamic 500
Questions
Frequently asked questions
How do I send samples for XRD Phase Analysis?
Fill in the analysis request form. Our team replies with preparation and shipping instructions for your sample type, and we confirm together that the sample is suitable before you send it.
How long does XRD Phase Analysis take?
It depends on the number of samples and laboratory workload. The estimated time on this page is a reference; once we review your request we share a firm schedule.
How is the price set?
The price on this page is a list price. It may change with the number of samples and any additional requests; after we agree the scope, the final price is shared in a proposal.
How do I receive the results?
Results are delivered as a written report. You can follow the status of your request in your account and through email notifications.
Can I request this from abroad?
Yes. We accept requests in Turkish, English, Arabic and Persian, and reply in the language you prefer.
Can I see your quality documents?
We develop our quality processes with reference to ISO/IEC 17025. For the current documents and scope details, contact us and we will send them in writing.
Instruments used
Spectroscopy and diffraction
Anton Paar XRDynamic 500 X-ray Diffractometer (XRD)
Crystalline phase identification, quantitative phase analysis, crystallite size and non-ambient structural studies on powders and solid materials.
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Sample preparation and processing
Milling and Particle Size Reduction
Planetary and high-energy ball milling for powder grinding, mechanical alloying, nanoscale size reduction and homogeneous blending of materials.
Training
Instrument Operator Training
Hands-on operator training on analytical instruments including SEM/EDS, XRD, Raman and rheometry, covering sample preparation, measurement and data interpretation.
Request this service
Describe your sample and the decision it supports. We reply with a technical proposal.